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Structure Determination Using Spectroscopic Methods
This note focuses on how spectroscopic techniques can be integrated to determine the structure of unknown molecules. It starts off with an overview of the electromagnetic spectrum and basic 1H NMR, moving on to much advanced discussion about how NMR can be combined with other methods such as IR, UV, and mass spectrometry for an overall structural analysis. It goes over chemical shifts of protons, coupling constants, and the use of 2D NMR for obtaining detailed structural information. Other topics discussed include multinuclear NMR, dynamic NMR and conformational, as well as chemical exchange rates measurement. This note is perfect for students and researchers who want to use several spectroscopic methods in the determination of the structure of a compound.
Author(s): Hans J. Reich
NA Pages 
This multi-topic resource covers key spectroscopy techniques used in the analysis of molecular and atomic systems. The note encompasses a detailed introduction to electronic spectroscopy, IR spectroscopy, and NMR spectroscopy, including both proton and carbon types, mass spectrometry, electron spin resonance (ESR), and Mössbauer spectroscopy. There is also a detailed description of every technique in its basic principles, experimental setup, and applications in different fields like chemistry, materials science, and biochemistry. The note also focuses on how these spectroscopic methods are applied to understand molecular structures, chemical bonding, and dynamic processes. Perfect for students and researchers, the book provides both a theoretical background and practical insights into the more general applications of spectroscopy in modern scientific research.
Author(s): Sathyabama Institute of Science and Technology
155 Pages
Understanding NMR Spectroscopy
James Keeler's note on NMR spectroscopy is rather solid in presenting principles of NMR along with its application to chemical structure analysis. It covers key topics like energy levels involved in NMR, the vector model, Fourier transformation, and data processing. The note explains how NMR spectrometers work and introduces more advanced techniques like two-dimensional NMR, which permits the analysis of far more detailed complex molecular structures. Additional topics covered include relaxation processes, phase cycling, and gradient pulses to give a full understanding of NMR spectroscopy to students and researchers looking to master this powerful analytical tool.
Author(s): James Keeler
NA Pages